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The Resource Fast scanning calorimetry, Christoph Schick, Vincent Mathot, editors, (electronic book)

Fast scanning calorimetry, Christoph Schick, Vincent Mathot, editors, (electronic book)

Label
Fast scanning calorimetry
Title
Fast scanning calorimetry
Statement of responsibility
Christoph Schick, Vincent Mathot, editors
Contributor
Subject
Language
eng
Summary
In the past decades, the scan rate range of calorimeters has been extended tremendously at the high end, from approximately 10 up to 10 000 000 °C/s and more. The combination of various calorimeters and the newly-developed Fast Scanning Calorimeters (FSC) now span 11 orders of magnitude, by which many processes can be mimicked according to the time scale(s) of chemical and physical transitions occurring during cooling, heating and isothermal stays in case heat is exchanged. This not only opens new areas of research on polymers, metals, pharmaceuticals and all kinds of substances with respect to glass transition, crystallization and melting phenomena, it also enables in-depth study of metastability and reorganization of samples on an 1 to 1000 ng scale. In addition, FSC will become a crucial tool for understanding and optimization of processing methods at high speeds like injection molding. The book resembles the state-of-the art in Thermal Analysis & Calorimetry and is an excellent starting point for both experts and newcomers in the field
Member of
Cataloging source
EBLCP
Dewey number
  • 536/.6
  • 620.11
Index
index present
LC call number
  • QC291
  • TA401-492
Literary form
non fiction
Nature of contents
dictionaries
http://library.link/vocab/relatedWorkOrContributorName
  • Schick, Christoph
  • Mathot, Vincent
http://library.link/vocab/subjectName
  • Calorimetry
  • Materials science
  • Polymers
  • Chemical engineering
  • Thermodynamics
  • Heat engineering
  • Heat
  • Mass transfer
  • Materials Science
  • Characterization and Evaluation of Materials
  • Engineering Thermodynamics, Heat and Mass Transfer
  • Polymer Sciences
  • Industrial Chemistry/Chemical Engineering
Label
Fast scanning calorimetry, Christoph Schick, Vincent Mathot, editors, (electronic book)
Instantiates
Publication
Note
  • 1.4.5.3 Cooling Rate Dependence of the Glass Transition
  • Includes index
Antecedent source
unknown
Carrier category
online resource
Carrier category code
cr
Carrier MARC source
rdacarrier
Color
multicolored
Content category
text
Content type code
txt
Content type MARC source
rdacontent
Contents
  • Preface; Contents; About the Editors; Part I: Advanced Instrumentation, Techniques and Methods; Chapter 1: Material Characterization by Fast Scanning Calorimetry: Practice and Applications; 1.1 Introduction; 1.2 Instrumental; 1.2.1 General Aspects; 1.2.1.1 The Calorimeter; 1.2.1.2 The Sample; 1.2.2 Design of the Flash DSC; 1.2.3 The Flash DSC Sensor; 1.2.3.1 Sensor Design; 1.2.3.2 Operation Mode; 1.2.3.3 Placing a Chip-Sensor into the Flash DSC; 1.2.4 Properties of the Flash DSC; 1.2.4.1 Possible Scanning Rates and Purge Gas; 1.2.4.2 Thermal Lag; 1.2.4.3 Isothermal Behavior
  • 1.2.4.4 Temperature Correction1.2.4.5 Dynamic Temperature Gradients; 1.2.4.6 Static Temperature Gradients; 1.2.4.7 Relation Between Scanning Rates and Sample Size; 1.2.5 Comments Regarding the Temperature Program; 1.2.6 Blank Correction; 1.2.6.1 The Blank Correction in Conventional DSC; 1.2.6.2 The Blank Correction in the Flash DSC; 1.2.6.3 Influence of Mechanical Interaction Between Sample and Sensor on the Measured Curve; 1.2.6.4 Reduction of the Mechanical Interaction; 1.3 Sample Preparation; 1.3.1 General Comments; 1.3.2 Polymers; 1.3.3 Low Molecular Organic Materials
  • 1.3.4 Metallic Glasses1.3.5 Estimation of the Sample Size; 1.3.5.1 Sample Size Estimation for Metallic Glass Alloys; 1.3.5.2 Sample Size Estimation for Polymers; Analyses of the Melting Peak; Analyses of the Glass Transition; Analyses of the Heat Capacity; Analyses of the Volume; 1.3.6 Determination of Sample Size Depending Effects (Critical Sample Size); 1.3.7 Measurements of the Initial Sample at the First Heating Run; 1.3.8 General Comments About the Use of Oil as a Contact Medium; 1.3.8.1 Selection and Behavior of Oil; 1.3.8.2 Application of an Oil Film
  • 1.3.8.3 Limitation of the Use of Silicone Oil as Contact Medium1.4 Concepts of Polymer Analysis; 1.4.1 Polymers Are Meta Stable Materials; 1.4.2 Measurement of Crystallization Effects; 1.4.2.1 General Comments; 1.4.2.2 Typical Temperature Programs; 1.4.2.3 Example: Influence of Nucleating Agents and Additives on the Crystallization of Poly(Butadiene Terephthalate) Polymers; 1.4.2.4 Example: Cold Crystallization of Isotactic Polypropylene; 1.4.3 Analyses of Melting Processes; 1.4.3.1 Reorganization During Heating; 1.4.3.2 Example: Reorganization of Isotactic Polypropylene
  • 1.4.3.3 Influence of the Heating Rate on the Temperature of Melting PeaksMelting of Stable Crystals Without Superheating; Melting of Stable Crystals with Superheating; 1.4.3.4 Example: Melting of Isotactic Polypropylene; 1.4.3.5 Example: Melting of Poly(Ethylene Terephthalate); 1.4.4 Investigation of Polymer Stability; 1.4.4.1 General Comments and Typical Temperature Programs; 1.4.4.2 Example: Stability of Poly(Etheretherketone); 1.4.5 Analysis of the Noncrystalline Fractions; 1.4.5.1 The Three-Phase Model; 1.4.5.2 Determination of the Amorphous Phases
Control code
SPR952934113
Dimensions
unknown
Extent
1 online resource (796 pages)
File format
unknown
Form of item
online
Isbn
9783319313290
Level of compression
unknown
Media category
computer
Media MARC source
rdamedia
Media type code
c
Other control number
10.1007/978-3-319-31329-0
Quality assurance targets
not applicable
Reformatting quality
unknown
Sound
unknown sound
Specific material designation
remote
Label
Fast scanning calorimetry, Christoph Schick, Vincent Mathot, editors, (electronic book)
Publication
Note
  • 1.4.5.3 Cooling Rate Dependence of the Glass Transition
  • Includes index
Antecedent source
unknown
Carrier category
online resource
Carrier category code
cr
Carrier MARC source
rdacarrier
Color
multicolored
Content category
text
Content type code
txt
Content type MARC source
rdacontent
Contents
  • Preface; Contents; About the Editors; Part I: Advanced Instrumentation, Techniques and Methods; Chapter 1: Material Characterization by Fast Scanning Calorimetry: Practice and Applications; 1.1 Introduction; 1.2 Instrumental; 1.2.1 General Aspects; 1.2.1.1 The Calorimeter; 1.2.1.2 The Sample; 1.2.2 Design of the Flash DSC; 1.2.3 The Flash DSC Sensor; 1.2.3.1 Sensor Design; 1.2.3.2 Operation Mode; 1.2.3.3 Placing a Chip-Sensor into the Flash DSC; 1.2.4 Properties of the Flash DSC; 1.2.4.1 Possible Scanning Rates and Purge Gas; 1.2.4.2 Thermal Lag; 1.2.4.3 Isothermal Behavior
  • 1.2.4.4 Temperature Correction1.2.4.5 Dynamic Temperature Gradients; 1.2.4.6 Static Temperature Gradients; 1.2.4.7 Relation Between Scanning Rates and Sample Size; 1.2.5 Comments Regarding the Temperature Program; 1.2.6 Blank Correction; 1.2.6.1 The Blank Correction in Conventional DSC; 1.2.6.2 The Blank Correction in the Flash DSC; 1.2.6.3 Influence of Mechanical Interaction Between Sample and Sensor on the Measured Curve; 1.2.6.4 Reduction of the Mechanical Interaction; 1.3 Sample Preparation; 1.3.1 General Comments; 1.3.2 Polymers; 1.3.3 Low Molecular Organic Materials
  • 1.3.4 Metallic Glasses1.3.5 Estimation of the Sample Size; 1.3.5.1 Sample Size Estimation for Metallic Glass Alloys; 1.3.5.2 Sample Size Estimation for Polymers; Analyses of the Melting Peak; Analyses of the Glass Transition; Analyses of the Heat Capacity; Analyses of the Volume; 1.3.6 Determination of Sample Size Depending Effects (Critical Sample Size); 1.3.7 Measurements of the Initial Sample at the First Heating Run; 1.3.8 General Comments About the Use of Oil as a Contact Medium; 1.3.8.1 Selection and Behavior of Oil; 1.3.8.2 Application of an Oil Film
  • 1.3.8.3 Limitation of the Use of Silicone Oil as Contact Medium1.4 Concepts of Polymer Analysis; 1.4.1 Polymers Are Meta Stable Materials; 1.4.2 Measurement of Crystallization Effects; 1.4.2.1 General Comments; 1.4.2.2 Typical Temperature Programs; 1.4.2.3 Example: Influence of Nucleating Agents and Additives on the Crystallization of Poly(Butadiene Terephthalate) Polymers; 1.4.2.4 Example: Cold Crystallization of Isotactic Polypropylene; 1.4.3 Analyses of Melting Processes; 1.4.3.1 Reorganization During Heating; 1.4.3.2 Example: Reorganization of Isotactic Polypropylene
  • 1.4.3.3 Influence of the Heating Rate on the Temperature of Melting PeaksMelting of Stable Crystals Without Superheating; Melting of Stable Crystals with Superheating; 1.4.3.4 Example: Melting of Isotactic Polypropylene; 1.4.3.5 Example: Melting of Poly(Ethylene Terephthalate); 1.4.4 Investigation of Polymer Stability; 1.4.4.1 General Comments and Typical Temperature Programs; 1.4.4.2 Example: Stability of Poly(Etheretherketone); 1.4.5 Analysis of the Noncrystalline Fractions; 1.4.5.1 The Three-Phase Model; 1.4.5.2 Determination of the Amorphous Phases
Control code
SPR952934113
Dimensions
unknown
Extent
1 online resource (796 pages)
File format
unknown
Form of item
online
Isbn
9783319313290
Level of compression
unknown
Media category
computer
Media MARC source
rdamedia
Media type code
c
Other control number
10.1007/978-3-319-31329-0
Quality assurance targets
not applicable
Reformatting quality
unknown
Sound
unknown sound
Specific material designation
remote

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